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Title: 1,2-dimetil-1,1,2,2-tetrafenildisilana Sulfonat Mengkatalisis Reaksi Esterifikasi Asam Stearat dengan Metanol dan 2-propanol
Authors: Bali, Paulus Osara
Advisors: Bangun, Nimpan
Sembiring, Seri Bima
Issue Date: 23-Feb-2015
Abstract: Esterification reaction between stearic acid with methanol and 2-propanol using 1,2-dimethyl-1,1,2,2-tetraphenyldisilane sulfonate as catalyst have gave methyl stearate and isopropyl stearate. Esterification reaction was carried in stainless steel reactor at 100oC for 10 hours with 1 : 6 molar ratio of oil to alcohol and 4 wt% catalyst. Product of esterification was characterized by FT-IR, gas chromatography, and nuclear magnetic resonance. The results showed that methyl stearate and isopropyl stearate have been made with yield 86.1 % and 67.5 %.
Abstract (other language): Reaksi esterifikasi antara asam stearat dengan metanol dan 2-propanol menggunakan katalis 1,2-dimetil-1,1,2,2-tetrafenildisilana sulfonat telah menghasilkan metil stearat dan isopropil stearat. Reaksi esterifikasi dilakukan dalam reaktor stainless steel pada suhu 100oC selama 10 jam dengan rasio mol asam stearat : alkohol = 1 : 6 dan jumlah katalis 4 %. Pengujian hasil esterifikasi dilakukan dengan spektroskopi FT-IR, Kromatografi Gas, dan spektroskopi 1H-NMR. Data yang diperoleh membuktikan bahwa metil stearat dan isopropil stearat telah terbentuk dengan yield masing-masing 86,1 % dan 67,5 %.
Keywords: 1,2-dimetil-1,1,2,2-tetrafenildisilana Sulfonat
Reaksi Esterifikasi
Asam Stearat
Appears in Collections:SP - Chemistry

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Abstract.pdfAbstract441.07 kBAdobe PDFView/Open
Chapter I.pdfChapter I451.4 kBAdobe PDFView/Open
Chapter II.pdfChapter II500.63 kBAdobe PDFView/Open
Chapter III-V.pdfChapter III-V1.75 MBAdobe PDFView/Open
Reference.pdfReference451.08 kBAdobe PDFView/Open
Appendix.pdfAppendix610.74 kBAdobe PDFView/Open

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