Steam Distillation Extraction Of 2,4,6- Tribromoanisole In Milk Sample And Analysis Using Gc-Ms In Ei+ Mode
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The application of a steam distillation extraction method for GC-MS detection of 2,4,6-tribromoanisole in milk product is described. The milk samples were extracted with hexane as the solvent for six hours. Mirex was used as the volumetric standard. The average recovery of the compound were 76-90%.The limit of detection was 1.74 μgL-1 .